PS Blister Inner Trays Crack Where Stress Meets a Sealing Solvent

PS Blister Inner Trays Crack Where Stress Meets a Sealing Solvent
Thin-wall forming: a production part is the only useful reference for a discussion about process drift.

PS blister inner trays craze and crack near formed corners after contact with a sealing or cleaning fluid, a classic environmental stress-cracking pattern.

What the failure looks like on the line

PS blister packs and trays are stiff and economical, and their failure mode is usually a crack or a stressed hinge rather than a slow distortion.

Fine cracks appear on PS blister cavities days after packing, clustered at high-stress corners and near the seal flange. The trays were sound at incoming inspection.

Forming leaves residual tensile stress in the PS at tight radii. Contact with an aggressive fluid or its vapour lets the stress relax by crazing, and the crazes grow into visible cracks. The combination of stress and fluid, not either alone, drives the failure.

The useful question is not whether the part conforms, but which condition was never written into the specification. On a buyer's specification this distinction matters: a part can measure inside tolerance and still fail in use, because the drawing records geometry while the complaint records behaviour. Corner radius is usually the first value both sides compare, and it is also the one most often quoted without the conditions attached to it.

The process window that decides it

Four variables move this result more than the rest. The ranges below are illustrative engineering guidance for a first discussion; confirm them on your own tool, material grade and part geometry before they become contract terms.

Variable Typical window What fails outside it
Corner radius 1.0-2.5 mm Tighter radii concentrate residual stress
Forming temperature 135-165 C Cold forming locks higher residual stress into PS
Post-formed relaxation time 0-24 h Short delay keeps stress high at packing
Fluid exposure index 0-2 h contact Longer contact grows crazes in stressed zones

Table 1. Starting window for a joint process trial. Values are engineering guidance, not a measured survey.

Corner radius is typically held at 1.0-2.5 mm. Tighter radii concentrate residual stress Record it together with the measurement point and the moment in the cycle; a single number without a location is not a process setting.

Forming temperature is typically held at 135-165 C. Cold forming locks higher residual stress into PS When this drifts, the symptom usually appears at one cavity, one sheet position or one lane before it appears across the whole batch.

Post-formed relaxation time is typically held at 0-24 h. Short delay keeps stress high at packing A change here is cheap during a trial and expensive after tooling release, so treat it as a controlled variable with a documented re-approval.

Fluid exposure index is typically held at 0-2 h contact. Longer contact grows crazes in stressed zones Put it on the change-control list, otherwise an unannounced material or setting substitution will be mistaken for ordinary process noise.

Reading the response curve

PS Blister Inner Trays Crack Where Stress Meets a Sealing Solvent: Uncracked trays (%) against Time after fluid contact (h)
Figure 1. Left: Uncracked trays (%) against Time after fluid contact (h). Right: how audited failures of this type typically split by cause. All plotted values are illustrative engineering guidance, not a measured survey.

The left panel shows uncracked trays (%) as time after fluid contact (h) increases: the response falls from 98 to 11 on the illustrative 0–100 scale. The dashed line at 60 marks a proposed acceptance limit, not a universal standard. Move that line only after the test method and the sample plan have been agreed, otherwise two suppliers can both be compliant and still deliver different parts.

Read the shape rather than a single point. A curve that changes quickly near the limit is more sensitive to ordinary process noise than one that approaches it gradually, and that difference should be reflected in how tightly the setting is controlled and how often it is checked.

Where the causes actually sit

The right panel of Figure 1 splits audited failures of this type into five groups. The percentages are illustrative engineering guidance for prioritising an investigation, not a measured survey and not a prediction for your line.

Cause Illustrative share First check
Residual forming stress 34% Mark the formed corner radii and look for crazing at those zones.
Tight corner radius 24% List any sealing, cleaning or printing fluids used near the tray.
Aggressive fluid contact 18% Compare cracked and uncracked trays from the same forming shift.
Cold-formed sheet 14% Hold formed trays before packing and note whether cracking is delayed.
Short relaxation time 10% Request the supplier material documentation and check its stated scope.

Table 2. Cause split and the corresponding first check. Shares are indicative and sum to 100.

Residual forming stress accounts for roughly 34% of the illustrative split. Mark the formed corner radii and look for crazing at those zones. Start here before authorising a material or tooling change, because it is the fastest explanation to confirm or eliminate.

Tight corner radius accounts for roughly 24% of the illustrative split. List any sealing, cleaning or printing fluids used near the tray. Start here before authorising a material or tooling change, because it is the fastest explanation to confirm or eliminate.

Aggressive fluid contact accounts for roughly 18% of the illustrative split. Compare cracked and uncracked trays from the same forming shift. Start here before authorising a material or tooling change, because it is the fastest explanation to confirm or eliminate.

Checks before sign-off

Work through these in order; measuring a later variable before an earlier one hides the cause rather than finding it.

  1. Mark the formed corner radii and look for crazing at those zones.
  2. List any sealing, cleaning or printing fluids used near the tray.
  3. Compare cracked and uncracked trays from the same forming shift.
  4. Hold formed trays before packing and note whether cracking is delayed.
  5. Request the supplier material documentation and check its stated scope.

Keep a retained reference sample beside every result. When a batch is disputed, the comparison that settles it is almost always between the retained part and the current one under the same method, not between either part and a number on a drawing. Record the instrument, the operator, the conditioning time and the position on the part or sheet for each reading.

Writing it into the specification and the evidence pack

Trays shall show no visible crazing or cracking at the defined high-stress zones after the agreed conditioning and fluid-exposure hold.

Write the requirement as a behaviour at a stated condition, not as a brand of material or a machine setting. State the test method, the conditioning, the sample plan and the rule for deciding a pass. Where a document is needed, ask the supplier for documentation that covers the actual construction and check its scope against your own market before approval; a document for the base material alone does not describe the finished part you are buying.

At first-article approval, freeze the drawing revision, the material and colour identification, the process window, the tool and cavity identification, and the inspection method. Any later change to grade, site, tool, or window should trigger a new first article rather than a paper waiver. Keep retained samples from the approved lot and from each production lot so that a future comparison is possible.

Evidence item What it must show
Approved drawing and revision The exact geometry and tolerances the decision applies to
Material and colour identification Grade, supplier, colour reference and any declared recycled content
Process window and change log The agreed settings and any deviation since approval
Inspection record and retained samples Method, conditions, results and a physical reference from the same lot

Table 3. Minimum evidence pack for a first-article decision and a later batch dispute.

None of the figures above should be read as a measured survey. They are engineering guidance for framing a joint trial; confirm them on your own tool, grade and geometry before they become contract terms.

Questions buyers ask

Is this a material problem or a process problem?

Forming leaves residual tensile stress in the PS at tight radii. Contact with an aggressive fluid or its vapour lets the stress relax by crazing, and the crazes grow into visible cracks. The combination of stress and fluid, not either alone, drives the failure. It is worth separating the two before a supplier changes a grade: hold the material constant for one controlled run, then move one setting at a time. If the symptom follows the setting, the material was never the cause.

Can corner radius be traded against cycle time?

Only within the window stated in Table 1, and only with a recorded trial. Tighter radii concentrate residual stress A faster cycle that sits outside the window usually moves the failure downstream, where it costs more to find.

What should be recorded at incoming inspection?

Keep the measurement, the method, the sample identity and the conditions together. Mark the formed corner radii and look for crazing at those zones. A result without its conditions cannot be compared with a later batch.

Does a change of PS require re-approval?

Treat any change to material grade, tool, site or process window as a change that needs a new first-article decision. For thin-wall forming work the drawing alone is not enough; the process route is part of what was approved.

How many samples are enough for a first-article decision?

There is no universal number. Sample across cavities, lanes, sheet positions or reel lengths so that the spread is visible, not just the average. Agree the sample plan and the acceptance rule with the supplier before the trial starts.

What belongs in the evidence pack?

The approved drawing and revision, the material and colour identification, the process window, the inspection method and results, the retained reference samples, and documentation covering the actual construction. Ask the supplier to state the scope of each document and check it against your own market.

Seeing this on a current thin-wall forming job?

Send the drawing, the material and grade, the process window you are running, and the point in the cycle or the shelf life where the fault appears. We will help you separate a material question from a process question and a specification question before anyone changes a tool.

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